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Expired Canadian patentCanada

Process for preparing aromatic fluorides

CA 1289152 C · Owner: Mallinckrodt, Inc. · Inventors: Cantrell, Gary L.

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Abstract From the Canadian patent

An improved process is disclosed for preparing aromatic fluorides by diazotization-fluorination in hydrogen fluoride wherein the diazotized reaction mixture includes an oxidizing agent such as nitrosonium ion from excess diazotization agent. The improvement includes prior to, decomposing the diazonium fluoride adding to the, diazotized reaction mixture a member selected from hydrazine, aromatic hydrazine, semi-carbazide thio-, semicarbazide, acid salts thereof sulfur dioxide, sodium, sulfite, and sodium bisulfite to remove at least a portion of the oxidizing agent. Urea was found to be ineffective.

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Listed from its CIPO record in Patent Yard's archive of Canadian patents past their term. Its claims, description and drawings are in the CIPO record and on Google Patents, and the Claude kit works from them.

Why it's free to use

  • Granted September 17, 1991. A Canadian patent filed before October 1, 1989 lasted 17 years from grant, so its term ended September 17, 2008.
  • We check Canadian rights only. A patent in its family in another country could still be in force: check its family on Google Patents.
FiledApril 6, 1988
GrantedSeptember 17, 1991
Term endedSeptember 17, 2008
Patent numberCA 1289152 C
Classification (IPC)C07C25/13 +2 more

Timeline

Timeline From CIPO dates

1989199119931995199719992001200320052007Application filedApril 6, 1988Patent grantedSep 17, 1991Term endedSep 17, 2008

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Everything on this page comes from the CIPO record linked above. Contains information licensed under the Open Government Licence – Canada.